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Beilstein J. Org. Chem. 2015, 11, 2171–2178, doi:10.3762/bjoc.11.235
Graphical Abstract
Scheme 1: Synthesis of [Ni(η1-Cp)(η5-Cp)(IMes)] (1) and [NiCl(Cp)(IMes)] (2).
Scheme 2: Synthesis of [NiCl(Cp)(ICy)] using conventional heating.
Scheme 3: Synthesis of (a) [NiCl(Cp)(ICy)] (3) and (b) [NiCl(Cp)(IDD)] (4) with microwave heating.
Figure 1: Molecular structures of complexes [NiCl(Cp)(ICy)] (3) (left) and [NiCl(Cp)(IDD)] (4) (right) as det...
Scheme 4: Model Suzuki–Miyaura reaction for the evaluation of the new complexes as cross-coupling pre-catalys...